(+)-methylphenyl(triphenylgermyl)fluorosilane

Base Information

Chemical Name:(+)-methylphenyl(triphenylgermyl)fluorosilane
CAS No.:86962-18-7
Molecular Formula:C₂₅H₂₃FGeSi
Molecular Weight:443.132
Hs Code.:

Synonyms:(+)-methylphenyl(triphenylgermyl)fluorosilane

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Chemical Property of (+)-methylphenyl(triphenylgermyl)fluorosilane

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Technology Process of (+)-methylphenyl(triphenylgermyl)fluorosilane

There total 1 articles about (+)-methylphenyl(triphenylgermyl)fluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 86962-17-6
(-)-methylphenyl(triphenylgermyl)methoxysilane

: 109-63-7
trifluoroborane diethyl ether

: 86962-18-7
(+)-methylphenyl(triphenylgermyl)fluorosilane

Guidance literature:: In diethyl ether; one equivalent of BF3*Et2O was added dropwise to a soln. of silane at room temp., N2 atm.; evapn. in vac., recrystn. (pentane);
DOI:10.1016/S0022-328X(00)98846-6

Reference yield: 82.0%

: 86962-18-7
(+)-methylphenyl(triphenylgermyl)fluorosilane

: 86962-06-3
(-)-methylphenyl(triphenylgermyl)silane

Guidance literature:: With diisobutylaluminium hydride; In hexane; to a soln. of i-Bu2AlH fluorosilane was added, room temp., N2 atm.; acid hydrolysis, extn., evapn. in vac.;
DOI:10.1016/S0022-328X(00)98846-6

Reference yield: 50.0%

: 86962-18-7
(+)-methylphenyl(triphenylgermyl)fluorosilane

: 14474-59-0
naphthalen-1-yl-lithium

: 86962-23-4
CH₃(C₆H₅)((C₆H₅)3Ge)Si(C₁₀H₇)

Guidance literature:: In diethyl ether; silane was treated with equiv. amt. of naphthyllithium, room temp., 3 h, N2 atm.; recrystn. (pentane, 0°C);
DOI:10.1016/S0022-328X(00)98846-6