dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

Base Information

Chemical Name:dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate
CAS No.:136035-16-0
Molecular Formula:C₃₃H₂₇NO₁₁S
Molecular Weight:645.643
Hs Code.:

Synonyms:dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

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Chemical Property of dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

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Technology Process of dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

There total 4 articles about dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-isothiazoline-4,5-dicarboxylate

: 136035-16-0
dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chlorobenzene; for 4.5h; Heating;
DOI:10.1080/15257779408013275

Reference yield: 8.0%

: 89873-12-1
5-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,3,4-oxathiazol-2-one

: 762-42-5
dimethyl acetylenedicarboxylate

: 136035-16-0
dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

Guidance literature:: at 140 ℃; for 144h;
DOI:10.1080/15257779408013275

Reference yield:

: 89873-12-1
5-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,3,4-oxathiazol-2-one

: 136035-16-0
dimethyl 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4,5-isothiazoledicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / 0.75 h / 200 °C

2: 85 percent / DDQ / chlorobenzene / 4.5 h / Heating

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chlorobenzene;
DOI:10.1080/15257779408013275