8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

Base Information

Chemical Name:8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one
CAS No.:1312558-06-7
Molecular Formula:C₁₅H₁₃N₃O₃S₂
Molecular Weight:347.419
Hs Code.:

Synonyms:8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

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Chemical Property of 8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

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Technology Process of 8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

There total 4 articles about 8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3959-23-7
benzenesulfonylacetic acid

: 185040-32-8
4-methylamino-2-methylthiopyrimidine-5-carboxaldehyde

: 1312558-06-7
8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: benzenesulfonylacetic acid; 4-methylamino-2-methylthiopyrimidine-5-carboxaldehyde; With acetic acid; benzylamine; Reflux;

With sodium hydrogencarbonate;

Reference yield:

: 17759-30-7
(4-methylamino-2-methylsulfanyl-pyrimidin-5-yl)-methanol

: 1312558-06-7
8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / chloroform

2: acetic acid / benzylamine / Reflux

With manganese(IV) oxide; acetic acid; benzylamine; In chloroform;

Reference yield:

: 76360-82-2
4-methylamino-2-methylsulfanyl-pyrimidine-5-carboxylic acid ethyl ester

: 1312558-06-7
8-methyl-2-(methylsulfanyl)-6-(phenylsulfonyl)pyrido[2,3-d]pyrimidin-7(8H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Cooling with acetone-dry ice

2: manganese(IV) oxide / chloroform

3: acetic acid / benzylamine / Reflux

With manganese(IV) oxide; lithium aluminium tetrahydride; acetic acid; benzylamine; In tetrahydrofuran; chloroform;