1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene

Base Information

• Chemical Name: 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene
• CAS No.: 1201909-59-2
• Molecular Formula: C₂₇H₂₂Cl₂
• Molecular Weight: 417.378

Synonyms:1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene

Chemical Property of 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene

Chemical Property:

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Technology Process of 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene

There total 2 articles about 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-bis(4-chlorophenyl)-2,2-dibromocyclopropane (22219-36-9) + hexa-1,5-dien-2-ylbenzene (7399-52-2) → 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene (1201909-59-2)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 36h;

DOI:10.1021/ol902505p DOI:10.1021/ol902832s

Reference yield:

1,1-bis(p-chlorophenyl)ethene (2642-81-1) → 1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene (1201909-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate / pentane

2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / tetrahydrofuran / 36 h / 20 °C

With potassium tert-butylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; pentane;

DOI:10.1055/s-0030-1259715

Reference yield: 91.0%

1-(2-(2-(but-3-enyl)-2-phenylcyclopropylidene)-1-(4-chlorophenyl)vinyl)-4-chlorobenzene (1201909-59-2) + diphenyl diselenide (1666-13-3) → C39H32Cl2Se2

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201103461

upstream raw materials:

1,1-bis(4-chlorophenyl)-2,2-dibromocyclopropane

hexa-1,5-dien-2-ylbenzene

1,1-bis(p-chlorophenyl)ethene

Downstream raw materials:

4-(2-(2,2-bis(4-chlorophenyl)vinylidene)-1-phenylcyclopropyl)butan-1-ol

C₂₇H₂₃BrCl₂O

C₂₇H₂₃Cl₂FO

C₃₉H₃₂Cl₂Se₂

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