O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Base Information

Chemical Name:O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate
CAS No.:1290140-08-7
Molecular Formula:C₂₃H₂₉NO₄S₂
Molecular Weight:447.62
Hs Code.:

Synonyms:O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Suppliers and Price of O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

There total 7 articles about O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 1290140-07-6
N-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]-2-methylpropane-2-amine

: 140-89-6
potassium ethyl xanthogenate

: 1290140-08-7
O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Guidance literature:: bis(trichloromethyl) carbonate; N-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]-2-methylpropane-2-amine; With triethylamine; In dichloromethane; at 0 - 0.35 ℃; for 0.166667h;

potassium ethyl xanthogenate; In acetonitrile; at 0.1 - 0.35 ℃; for 0.25h;

Reference yield:

: C₂₀H₂₄ClNO₃

: 140-89-6
potassium ethyl xanthogenate

: 1290140-08-7
O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Guidance literature:: In acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1016/j.tet.2011.01.003

Reference yield:

: 90-02-8
salicylaldehyde

: 1290140-08-7
O-ethyl [tert-butyl-[[2-[(4-methoxyphenyl)methoxy]phenyl]methyl]carbamoyl]sulfanylmethanethioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 12 h / Reflux

2.1: methanol / 12 h / 20 °C / Molecular sieve

2.2: 0.5 h / Cooling with ice

3.1: triethylamine / dichloromethane / 0 - 20 °C

4.1: acetonitrile / 0.25 h / 20 °C

With potassium carbonate; triethylamine; In methanol; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.tet.2011.01.003