Technology Process of C28H30N2O7S
There total 10 articles about C28H30N2O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
methanol; dichloromethane;
at 100 ℃;
for 0.5h;
Sealed tube;
Microwave Irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / N,N-dimethyl-formamide / Inert atmosphere
1.2: 6 h / 75 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / -30 - 20 °C
3.1: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 70 °C
4.1: gold(III) chloride / trifluoroacetic acid / 0.75 h / 100 °C / Sealed tube; Microwave Irradiation
5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / methanol; dichloromethane / 0.5 h / 100 °C / Sealed tube; Microwave Irradiation
With
copper(l) iodide; tetrabutyl ammonium fluoride; sodium carbonate; triethylamine;
gold(III) chloride; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0); triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; trifluoroacetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 20 °C
2: copper(l) iodide; triethylamine / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 2 h / 70 °C
3: gold(III) chloride / trifluoroacetic acid / 0.75 h / 100 °C / Sealed tube; Microwave Irradiation
4: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / methanol; dichloromethane / 0.5 h / 100 °C / Sealed tube; Microwave Irradiation
With
copper(l) iodide; sodium carbonate; potassium carbonate; triethylamine;
gold(III) chloride; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium(0);
In
methanol; dichloromethane; N,N-dimethyl-formamide; acetone; trifluoroacetic acid;