1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

Base Information

Chemical Name:1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate
CAS No.:1434880-46-2
Molecular Formula:C₂₀H₂₀Br₂N₂O₂
Molecular Weight:480.199
Hs Code.:

Synonyms:1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

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Chemical Property of 1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

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Technology Process of 1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

There total 3 articles about 1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 874184-69-7
1 ,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride

: 124-38-9,18923-20-1
carbon dioxide

: 1434880-46-2
1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

Guidance literature:: 1 ,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium chloride; With potassium hexamethylsilazane; In tetrahydrofuran; for 0.166667h; Inert atmosphere; Glovebox;

carbon dioxide; In tetrahydrofuran; for 0.0333333h; Inert atmosphere; Glovebox;
DOI:10.1021/ja401965d

Reference yield:

: 24596-19-8
4-bromo-2,6-dimethylphenylamine

: 1434880-46-2
1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 12 h / 140 °C

2.1: N-ethyl-N,N-diisopropylamine / 72 h / 120 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran / 0.17 h / Inert atmosphere; Glovebox

3.2: 0.03 h / Inert atmosphere; Glovebox

With potassium hexamethylsilazane; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja401965d

Reference yield:

: 1351288-11-3
N,N’-bis(4-bromo-2,6-dimethylphenyl)formimidamide

: 1434880-46-2
1,3-bis(4-bromo-2,6-dimethylphenyl)-4,5-dihydro-1H-imidazol-3-ium-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / 72 h / 120 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.17 h / Inert atmosphere; Glovebox

2.2: 0.03 h

With potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;