4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

Base Information

Chemical Name:4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate
CAS No.:1346570-35-1
Molecular Formula:C₁₉H₁₅ClN₂O₄
Molecular Weight:370.792
Hs Code.:

Synonyms:4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

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Chemical Property of 4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

Chemical Property:

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Technology Process of 4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

There total 6 articles about 4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1346570-34-0
4-(1-(4-chlorophenyl)-3-hydrazinyl-3-oxoprop-1-en-2-yl)phenyl ethyl carbonate

: 122-51-0
orthoformic acid triethyl ester

: 1346570-35-1
4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

Guidance literature:: With toluene-4-sulfonic acid; at 90 - 100 ℃; for 2h;

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1346570-35-1
4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / 3 h / Reflux

1.2: 0.5 h / Reflux

2.1: sulfuric acid / 16 h / Reflux

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 0.25 h / 22 - 26 °C

3.2: Acidic conditions

4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

4.2: 1 h / 0 °C

5.1: toluene-4-sulfonic acid / 2 h / 90 - 100 °C

With sulfuric acid; water; toluene-4-sulfonic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; 1.1: Perkin Reaction;

Reference yield:

: 156-38-7
4-hydroxyphenylacetate

: 1346570-35-1
4-[2-(4-chlorophenyl)-1-(1,3,4-oxadiazol-2-yl)ethenyl]phenyl ethyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / 3 h / Reflux

1.2: 0.5 h / Reflux

2.1: sulfuric acid / 16 h / Reflux

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 0.25 h / 22 - 26 °C

3.2: Acidic conditions

4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

4.2: 1 h / 0 °C

5.1: toluene-4-sulfonic acid / 2 h / 90 - 100 °C

With sulfuric acid; water; toluene-4-sulfonic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; 1.1: Perkin Reaction;