tetramethylbutatriene(hexacarbonyl)diirion

Base Information

Chemical Name:tetramethylbutatriene(hexacarbonyl)diirion
CAS No.:12212-46-3
Molecular Formula:C₁₄H₁₂Fe₂O₆
Molecular Weight:387.94
Hs Code.:

Synonyms:tetramethylbutatriene(hexacarbonyl)diirion

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethylbutatriene(hexacarbonyl)diirion

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of tetramethylbutatriene(hexacarbonyl)diirion

There total 1 articles about tetramethylbutatriene(hexacarbonyl)diirion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 40747-47-5
[Co2(CO)6(μ-η(2),η(2)-HOC(CH3)2CCC(CH3)2OH)]

: 17685-52-8
triiron dodecarbonyl

: 12212-46-3
tetramethylbutatriene(hexacarbonyl)diirion

: FeCo(CO)6((CH₃)2CC₂C(CH₃)2OH)

Guidance literature:: In acetone; under N2 Co2(CO)6(HOMe2CC2CMe2OH) and Fe(CO)5 refluxed in acetone for 10 h; mixt. cooled and filtered, solvent removed in vacuo, residue dissolved in CH2Cl2 and chromed. on tlc preparative plates, eluant light petroleumand 10% diethyl ether; elem. anal.;
DOI:10.1016/S0277-5387(00)84676-8

Reference yield: 47.0%

: 12212-46-3
tetramethylbutatriene(hexacarbonyl)diirion

: 25299-08-5
diisopropylidenesuccinic anhydride

: 142-30-3
2,5-dihydroxy-2,5-dimethyl-3-hexyne

Guidance literature:: With carbon monoxide; water; In water; acetonitrile; benzene; addn. of CAN to soln. of cumulene complex in alcohol and benzene, bubbling of CO, stirred for 4h at room temp.; diln with H2O, extn. (Et2O), chromy. (silica gel);
DOI:10.1246/cl.1988.891

Reference yield: 24.0%

: 12212-46-3
tetramethylbutatriene(hexacarbonyl)diirion

: 17997-36-3
2,5-diethoxy-2,5-dimethyl-hex-3-yne

: 22769-97-7
diethyl 2,3-diisopropylidene-succinate

Guidance literature:: With ethanol; carbon monoxide; In ethanol; benzene; addn. of CAN to soln. of cumulene complex in alcohol and benzene, bubbling of CO, stirred for 4h at room temp.; diln with H2O, extn. (Et2O), chromy. (silica gel);
DOI:10.1246/cl.1988.891