methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

Base Information

Chemical Name:methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate
CAS No.:669062-19-5
Molecular Formula:C₃₀H₂₉IN₂O₆S
Molecular Weight:672.541
Hs Code.:

Synonyms:methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

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Chemical Property of methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

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Technology Process of methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

There total 8 articles about methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 669062-18-4
4-iodo-N-(prop-2-ynyl)benzenesulfonamide

: 669062-17-3
methyl N-(3-(chloromethyl)benzoyl)-2-(-2-propen-1-yloxy)phenylalaninate

: 669062-19-5
methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo0352629

Reference yield:

: 63024-77-1
3-(Chloromethyl)benzoyl chloride

: 669062-19-5
methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.536 g / Et₃N / CH₂Cl₂ / 4 h / 0 °C

2: 87 percent / NaH / dimethylformamide

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0352629

Reference yield:

: 98-61-3
p-Iodobenzenesulfonyl chloride

: 669062-19-5
methyl N-(3-(N-(2-propyn-1-yl)(4-iodophenyl)sulfonamidomethyl)benzoyl)(2-(2-propen-1-yloxy)phenyl)alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Et₃N / CH₂Cl₂ / 20 h / 0 °C

2: 87 percent / NaH / dimethylformamide

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0352629