methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

Base Information

Chemical Name:methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside
CAS No.:405145-64-4
Molecular Formula:C₂₄H₃₂O₆SSi
Molecular Weight:476.666
Hs Code.:

Synonyms:methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

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Chemical Property of methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

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Technology Process of methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

There total 3 articles about methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 87316-20-9
methyl α-D-6-O-t-butyldiphenylsilyl-2,3-dideoxyhex-2-enoerythropyranoside

: 124-63-0
methanesulfonyl chloride

: 405145-64-4
methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

Guidance literature:: With dmap; triethylamine; In ethyl acetate; at 0 ℃; for 3h;
DOI:10.1016/S0957-4166(01)00450-5

Reference yield:

: 22860-25-9
methyl 2,3-dideoxy-4,6-dihydroxy-α-D-erythro-hex-2-enopyranoside

: 405145-64-4
methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine; DMAP / CH₂Cl₂ / 2 h / 0 °C

2: 86 percent / triethylamine; N,N-dimethylaminopyridine / ethyl acetate / 3 h / 0 °C

With dmap; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/S0957-4166(01)00450-5

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 405145-64-4
methyl α-D-6-O-t-butyldiphenylsilyl-4-O-methanesulphonyl-2,3-dideoxyhex-2-enoerythropyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / triethylamine; DMAP / CH₂Cl₂ / 2 h / 0 °C

2: 86 percent / triethylamine; N,N-dimethylaminopyridine / ethyl acetate / 3 h / 0 °C

With dmap; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/S0957-4166(01)00450-5