2-(2-chlorophenyl)-N,N-diethylethaneselenoamide

Base Information

• Chemical Name: 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide
• CAS No.: 1360685-03-5
• Molecular Formula: C₁₂H₁₆ClNSe
• Molecular Weight: 288.679
• Mol file: 1360685-03-5.mol

Synonyms:2-(2-chlorophenyl)-N,N-diethylethaneselenoamide

Chemical Property of 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide

There total 3 articles about 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

4-(2-chlorophenyl)-1,2,3-selenadiazole (1360685-01-3) + diethylamine (109-89-7) → 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide (1360685-03-5)

Guidance literature:

With potassium hydroxide; at 56 - 58 ℃; Inert atmosphere;

DOI:10.1134/S1070428012010265

Reference yield:

2'-chloroacetophenone semicarbazone → 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide (1360685-03-5)

Guidance literature:

Multi-step reaction with 2 steps

1: selenium(IV) oxide / acetic acid / 4 h / 65 °C

2: potassium hydroxide / 55 °C

With selenium(IV) oxide; potassium hydroxide; In acetic acid;

DOI:10.1021/ol400547n

Reference yield:

1-(2-chlorophenyl)ethanone (2142-68-9) → 2-(2-chlorophenyl)-N,N-diethylethaneselenoamide (1360685-03-5)

Guidance literature:

Multi-step reaction with 3 steps

1: Heating

2: selenium(IV) oxide; acetic acid / 5.5 h / 20 - 68 °C / Darkness

3: potassium hydroxide / 56 - 58 °C / Inert atmosphere

With selenium(IV) oxide; acetic acid; potassium hydroxide;

DOI:10.1134/S1070428012010265

upstream raw materials:

4-(2-chlorophenyl)-1,2,3-selenadiazole

diethylamine

1-(2-chlorophenyl)ethanone