N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine

Base Information

• Chemical Name: N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine
• CAS No.: 861529-65-9
• Molecular Formula: C₁₇H₁₉N₅O₄
• Molecular Weight: 357.369

Synonyms:N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine

Chemical Property of N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine

Chemical Property:

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Technology Process of N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine

There total 2 articles about N¹-(2,4-dinitro-benzylidene)-N²,N²,N⁴,N⁴-tetramethyl-benzene-1,2,4-triyltriamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N,N',N'-tetramethyl-m-phenylenediamine (22440-93-3) → N1-(2,4-dinitro-benzylidene)-N2,N2,N4,N4-tetramethyl-benzene-1,2,4-triyltriamine (861529-65-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diluted hydrochloric acid; sodium nitrite / in eiskaltem Wasser aufschwemmt, abwechselnd Natronlauge hizufuegt und mit Essigester ausschuettelt

2: alcohol; natrium carbonate

With hydrogenchloride; ethanol; sodium carbonate; sodium nitrite;

Reference yield:

2,4-dinitrotoluene (121-14-2) + tetra-N-methyl-4-nitroso-m-phenylenediamine (52695-14-4) → N1-(2,4-dinitro-benzylidene)-N2,N2,N4,N4-tetramethyl-benzene-1,2,4-triyltriamine (861529-65-9)

Guidance literature:

With ethanol; sodium carbonate;

Reference yield:

N1-(2,4-dinitro-benzylidene)-N2,N2,N4,N4-tetramethyl-benzene-1,2,4-triyltriamine (861529-65-9) → 2,4-dinitrobenzaldehyde (528-75-6)

Guidance literature:

upstream raw materials:

2,4-dinitrotoluene

tetra-N-methyl-4-nitroso-m-phenylenediamine

N,N,N',N'-tetramethyl-m-phenylenediamine

Downstream raw materials:

2,4-dinitrobenzaldehyde

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