Ethyl 10-methylphenanthrene-9-carboxylate

Base Information

Chemical Name:Ethyl 10-methylphenanthrene-9-carboxylate
CAS No.:232611-22-2
Molecular Formula:C18H16 O2
Molecular Weight:264.324
Hs Code.:
DSSTox Substance ID:DTXSID90571875
Nikkaji Number:J1.151.521E
Wikidata:Q82460058
Mol file:232611-22-2.mol

Synonyms:ethyl 10-methylphenanthrene-9-carboxylate;232611-22-2;ETHYL 10-METHYL-9-PHENANTHRENECARBOXYLATE;DTXSID90571875

Suppliers and Price of Ethyl 10-methylphenanthrene-9-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ETHYL-10-METHYL-9-PHENANTHRENECARBOXYLATE 95.00%
5MG
$ 501.51

Total 2 raw suppliers

Chemical Property of Ethyl 10-methylphenanthrene-9-carboxylate

Chemical Property:

Melting Point:88-89 °C
Boiling Point:422.7±14.0 °C(Predicted)
PSA：26.30000
Density:1.157±0.06 g/cm3(Predicted)
LogP:4.47810
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:264.115029749
Heavy Atom Count:20
Complexity:351

Purity/Quality:

98% ^*data from raw suppliers

ETHYL-10-METHYL-9-PHENANTHRENECARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(C2=CC=CC=C2C3=CC=CC=C31)C

Technology Process of Ethyl 10-methylphenanthrene-9-carboxylate

There total 2 articles about Ethyl 10-methylphenanthrene-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 4341-76-8
Ethyl 2-butynoate

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 217-59-4
triphenylene

: 232611-22-2
9-ethyl 10-methylphenanthrene-9-carboxylate

: 2,4-dimethyl-naphthalene-1,3-dicarboxylic acid diethyl ester

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; cesium fluoride; In acetonitrile; Ambient temperature;
DOI:10.1021/ja9907111

Reference yield: 52.0%

: 2178-24-7
ethyl 2-(2-bromophenyl)ethanoate

: 308103-40-4
(2-acetylphenyl)boronic acid

: 232611-22-2
9-ethyl 10-methylphenanthrene-9-carboxylate

Guidance literature:: With caesium carbonate; DavePhos; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene; at 120 - 150 ℃; for 0.166667h; microwave irradiation;
DOI:10.1021/jo702001n