12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

Base Information

Chemical Name:12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine
CAS No.:854758-08-0
Molecular Formula:C₅₉H₇₉N₅O₁₀Si
Molecular Weight:1046.39
Hs Code.:

Synonyms:12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

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Chemical Property of 12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

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Technology Process of 12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

There total 4 articles about 12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 854757-96-3
12'-iodo-3-(tert-butyl-dimethylsilanyloxy)vinblastine

: 104-94-9
4-methoxy-aniline

: 854758-08-0
12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

Guidance literature:: With sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 80 ℃; for 4h;

Reference yield:

: 90012-97-8
10'-iodovinblastine

: 854758-08-0
12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

2: sodium t-butanolate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 4 h / 80 °C

With N-ethyl-N,N-diisopropylamine; sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; toluene;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 854758-08-0
12'-(4-methoxyphenylamino)-3-(tert-butyl-dimethylsilanyloxy)vinblastine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h

2: sodium t-butanolate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 4 h / 80 °C

With N-ethyl-N,N-diisopropylamine; sodium t-butanolate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; toluene;