(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:1548723-15-4
Molecular Formula:C₂₆H₃₅NO₁₃
Molecular Weight:569.563
Hs Code.:

Synonyms:(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 6 articles about (2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1548723-11-0
C₄₄H₄₅F₁₇N₂O₁₆

: 1548723-15-4
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: In toluene; for 1h; UV-irradiation;
DOI:10.1021/ol500023y

Reference yield: 71.6%

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 145881-74-9
2-<2-N-(benzyloxycarbonyl)aminoethoxy>ethanol

: 1548723-15-4
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -5 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.ejmech.2020.112509

Reference yield:

: 1548722-88-8
C₃₀H₂₇F₁₇N₂O₇

: 1548723-15-4
(2R,3R,4S,5R,6S)-2-(acetoxymethyl)-6-(2-(2-(((benzyloxy)carbonyl)amino)ethoxy) ethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 2 h / 25 °C

1.2: 16 h / 25 °C

2.1: toluene / 1 h / UV-irradiation

In dichloromethane; toluene;
DOI:10.1021/ol500023y