(C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

Base Information

Chemical Name:(C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)
CAS No.:109956-78-7
Molecular Formula:C₁₂H₁₂FeO₄
Molecular Weight:276.072
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)(CO)2Fe(CHCHCO<sub>2</sub>C<sub>2</sub>H<sub>5</sub>)

Synonyms:(C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

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Chemical Property of (C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

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Technology Process of (C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

There total 2 articles about (C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 109864-35-9
((C₅H₅)(CO)Fe)2(CO)(CHCHCO₂C₂H₅)⁽¹⁺⁾*PF₆^(1-)=((C₅H₅)(CO)Fe)2(CO)(CHCHCO₂C₂H₅)PF₆

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 12078-28-3,38979-86-1
dicarbonylcyclopentadienyliodoiron(II)

: 109956-78-7
(C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

Guidance literature:: With carbon monoxide; In acetone; Fe-complex and NaI were stirred in acetone under a CO (0.65 atm) atmosphere for 10 min at -78°C and then 90 min at room temp.; evapd. in vacuo, Et2O was added, mixt. was filtered, filtrate evapd., residue was subjected to flash chromy. (Al2O3, Et2O-hexane); CpFe(CO)2I was identified by (1)H NMR and IR; high-resolution MS data for the alkenyl complex;

Reference yield: 23.0%

: 109864-35-9
((C₅H₅)(CO)Fe)2(CO)(CHCHCO₂C₂H₅)⁽¹⁺⁾*PF₆^(1-)=((C₅H₅)(CO)Fe)2(CO)(CHCHCO₂C₂H₅)PF₆

: 102-54-5,55404-68-7
ferrocene

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 38834-26-3
(η5-Cp)Fe(CO)3PF6

: 109956-78-7
(C₅H₅)(CO)2Fe(CHCHCO₂C₂H₅)

: 109864-36-0
((C₅H₅)(CO)Fe)2(CO)(CCHCO₂C₂H₅)

Guidance literature:: In [⁽²⁾H₆]acetone; thermal decomposition above -20°C; flash chromy. (alumina, CH2Cl2-hexane); high-resolution mass spectral data for (Cp(CO)Fe)2(μ-CO)(μ-C=CHCOOEt);