3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

Base Information

Chemical Name:3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione
CAS No.:1631037-66-5
Molecular Formula:C₂₆H₂₅N₅O₅S
Molecular Weight:519.581
Hs Code.:

Synonyms:3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

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Chemical Property of 3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

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Technology Process of 3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

There total 2 articles about 3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 110-91-8,99108-56-2
morpholine

: 910912-86-6
C₁₉H₁₂N₄O₄S

: 109-64-8
1,3-dibromo-propane

: 1631037-66-5
3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

Guidance literature:: C₁₉H₁₂N₄O₄S; 1,3-dibromo-propane; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

morpholine; With potassium hydroxide; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1002/ardp.201300466

Reference yield:

: 333327-63-2
3?( 3?nitrophenyl)-1?phenyl?1H?pyrazole?4?carbaldehyde

: 1631037-66-5
3-(3-morpholinopropyl)-5-((3-(3-nitrophenyl)-1-phenyl-1H-pyrazol-4-yl)methylene)thiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperidine / toluene / Reflux

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 90 °C

With piperidine; potassium hydroxide; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/ardp.201300466