9-benzyl-10-cyanoanthracene

Base Information

Chemical Name:9-benzyl-10-cyanoanthracene
CAS No.:72948-58-4
Molecular Formula:C₂₂H₁₅N
Molecular Weight:293.368
Hs Code.:

Synonyms:9-benzyl-10-cyanoanthracene

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Chemical Property of 9-benzyl-10-cyanoanthracene

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Technology Process of 9-benzyl-10-cyanoanthracene

There total 8 articles about 9-benzyl-10-cyanoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1217-45-4
9,10-Dicyanoanthracene

: 1539-57-7
diethyl 2,6-dimethyl-4-benzyl-1,4-dihydropyridine-3,5-dicarboxylate

: 72948-58-4
9-benzyl-10-cyanoanthracene

Guidance literature:: With tris[2-phenylpyridinato-C₂,N]iridium(III); sodium acetate; at 25 ℃; for 40h; Irradiation;
DOI:10.1002/cctc.201600037

Reference yield: 48.0%

: 1217-45-4
9,10-Dicyanoanthracene

: 28493-54-1
benzyltributyltin

: 72948-58-4
9-benzyl-10-cyanoanthracene

: 813-19-4
bis(tri-n-butyltin)

: 9-cyano-10-(tri-n-butyl stannyl)anthracene

Guidance literature:: In benzene; byproducts: bibenzyl; Irradiation (UV/VIS); 4.75 h irradn.; concg.; triturating with cold methanol; filtering; filtrate concg.; chromy. (alumina) eluting with CHCl3/petroleum; two fractions rechromy. (silica) with petroleum ether;
DOI:10.1021/ja00414a033

Reference yield: 3.0%

: 1217-45-4
9,10-Dicyanoanthracene

: 28493-54-1
benzyltributyltin

: 72948-58-4
9-benzyl-10-cyanoanthracene

: 813-19-4
bis(tri-n-butyltin)

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

: 9-cyano-10-(tri-n-butyl stannyl)anthracene

Guidance literature:: In benzene; Mechanism; Rate constant; Irradiation; kinetic parameters for the photoreactions with other p-XC₆H₄CH₂SnBu₃ (X = Cl, F, Me, MeO);
DOI:10.1021/ja00529a081