intermediate 6b

Base Information

• Chemical Name: intermediate 6b
• CAS No.: 842129-08-2
• Molecular Formula: C₂₁H₁₈FN₇O
• Molecular Weight: 403.419

Synonyms:intermediate 6b

Chemical Property of intermediate 6b

Chemical Property:

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Technology Process of intermediate 6b

There total 2 articles about intermediate 6b which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

intermediate 6a (840534-36-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → intermediate 6b (842129-08-2)

Guidance literature:

In DMF (N,N-dimethyl-formamide); at 20 - 115 ℃;

Reference yield: 17.0%

intermediate 6a (840534-36-3) + ethanol (64-17-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → intermediate 6b (842129-08-2) + intermediate 6c (842129-10-6)

Guidance literature:

With diethylamine; at 110 - 140 ℃;

Reference yield: 82.0%

intermediate 6b (842129-08-2) + 1-methylguanidine (471-29-4) → compound 34 (842127-68-8)

Guidance literature:

With sodium methylate; In 2-ethoxy-ethanol; for 4.5h; Heating / reflux;

upstream raw materials:

intermediate 6a

ethanol

N,N-dimethyl-formamide

Downstream raw materials:

compound 34

compound 22

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