(4-chlorophenylthio)methylthiirane

Base Information

Chemical Name:(4-chlorophenylthio)methylthiirane
CAS No.:36734-62-0
Molecular Formula:C₉H₉ClS₂
Molecular Weight:216.755
Hs Code.:

Synonyms:(4-chlorophenylthio)methylthiirane

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Chemical Property of (4-chlorophenylthio)methylthiirane

Chemical Property:

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Technology Process of (4-chlorophenylthio)methylthiirane

There total 2 articles about (4-chlorophenylthio)methylthiirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 5296-23-1
(4-chloro-phenylsulfanylmethyl)-oxirane

: 36734-62-0
(4-chlorophenylthio)methylthiirane

Guidance literature:: With potassium thioacyanate; In water; at 40 ℃; for 24h;
DOI:10.1039/c6ob02387h

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 36734-62-0
(4-chlorophenylthio)methylthiirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol / 0.33 h / 20 °C

1.2: 24 h / 20 °C

2.1: potassium thioacyanate / water / 24 h / 40 °C

With potassium thioacyanate; sodium hydroxide; In ethanol; water;
DOI:10.1039/c6ob02387h

Reference yield: 18.0%

: 36734-62-0
(4-chlorophenylthio)methylthiirane

: 1774-47-6
trimethylsulfoxonium iodide

: 2-(4-chlorophenylthiomethyl)thietane

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In tetrahydrofuran; at 40 ℃; for 3h;

(4-chlorophenylthio)methylthiirane; In tetrahydrofuran; dimethyl sulfoxide; at 40 ℃; for 4h;
DOI:10.1039/c6ob02387h