3,5-dimethoxyphenylzinc chloride

Base Information

Chemical Name:3,5-dimethoxyphenylzinc chloride
CAS No.:1260433-81-5
Molecular Formula:C₈H₉ClO₂Zn
Molecular Weight:238.001
Hs Code.:

Synonyms:3,5-dimethoxyphenylzinc chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-dimethoxyphenylzinc chloride

Chemical Property:

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Technology Process of 3,5-dimethoxyphenylzinc chloride

There total 1 articles about 3,5-dimethoxyphenylzinc chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20469-65-2
1-bromo-3,5-dimethoxybenzene

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1260433-81-5
3,5-dimethoxyphenylzinc chloride

Guidance literature:: With magnesium; lithium chloride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1002/anie.201510665

Reference yield: 89.0%

: 935-50-2
4,4-dimethoxycyclohexa-2,5-dienone

: 1260433-81-5
3,5-dimethoxyphenylzinc chloride

: 1260433-72-4
(R)-4,4-dimethoxy-5-(3,5-dimethoxyphenyl)-2-cyclohexenone

Guidance literature:: 4,4-dimethoxycyclohexa-2,5-dienone; 3,5-dimethoxyphenylzinc chloride; With chloro-trimethyl-silane; chlorobis(ethylene)rhodium(I) dimer; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In tetrahydrofuran; at -10 ℃; Inert atmosphere;

With ammonium hydroxide; water; In tetrahydrofuran; at -10 - 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja108717r

Reference yield: 86.0%

: 1108736-78-2
2-bromo-4-(4-chlorophenyl)pyrimidine

: 1260433-81-5
3,5-dimethoxyphenylzinc chloride

: 4-(4-chlorophenyl)-2-(3,5-dimethoxyphenyl)pyrimidine

Guidance literature:: With Li₂CoCl₄; sodium formate; In tetrahydrofuran; at 25 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201510665