Technology Process of 6-deoxy-6-C-(2'-ethanoic acid)-1,2,3,4,5-O-penta-O-benzyl-D-myo-inositol
There total 4 articles about 6-deoxy-6-C-(2'-ethanoic acid)-1,2,3,4,5-O-penta-O-benzyl-D-myo-inositol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
DOI:10.1039/c3ob41337c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ozone / methanol; dichloromethane / -78 °C
1.2: 2 h / -78 - 20 °C
2.1: sodium dihydrogenphosphate; sodium chlorite / water; tetrahydrofuran / 2 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; ozone;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c3ob41337c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C / Inert atmosphere
1.2: 0.5 h / 0 - 20 °C
2.1: ozone / methanol; dichloromethane / -78 °C
2.2: 2 h / -78 - 20 °C
3.1: sodium dihydrogenphosphate; sodium chlorite / water; tetrahydrofuran / 2 h / 20 °C
With
sodium chlorite; sodium dihydrogenphosphate; tetra-(n-butyl)ammonium iodide; sodium hydride; ozone;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c3ob41337c
