2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one

Base Information

• Chemical Name: 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one
• CAS No.: 25105-59-3
• Molecular Formula: C₁₀H₁₂N₂O₂
• Molecular Weight: 192.217

Synonyms:2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one

Chemical Property of 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one

Chemical Property:

Purity/Quality:

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Technology Process of 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one

There total 4 articles about 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

propylamine (107-10-8,42939-71-9) + 4-nitrobenzaldehdye (555-16-8) → 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one (25105-59-3)

Guidance literature:

In toluene; for 1h; Ambient temperature;

DOI:10.1002/jhet.5570330136

Reference yield:

4-nitrobenzaldehdye (555-16-8) → 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one (25105-59-3) + trans-3-nitro-2-(4-nitrophenyl)-1-propylaziridine

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate

2: N-chloro-succinimide; caesium carbonate / tetrahydrofuran / 5 h / 20 °C

With N-chloro-succinimide; ammonium acetate; caesium carbonate; In tetrahydrofuran;

DOI:10.1021/acs.orglett.7b02724

Reference yield:

→ 2,3,6,7-tetrahydro-2-(4-nitrophenyl)-3-propylcyclopenta-[e][1,3]oxazin-4(5H)-one (25105-59-3)

Guidance literature:

p-Nitrobenzaldehyd, n-Propylamin;

DOI:10.1246/bcsj.45.3179

upstream raw materials:

propylamine

4-nitrobenzaldehdye

1-nitro-4-[(E)-2-nitroeth-1-enyl]benzene

Downstream raw materials:

(E)-1-nitro-4-(2-nitro-2-phenylvinyl)benzene

3-methyl-5-(4-nitro-phenyl)-4-propyl-4,5-dihydro-[1,2,4]oxadiazole

3-(4-nitro-phenyl)-2-propyl-oxaziridine

3-bromo-2-(4-nitrophenyl)-4-oxo-1-propylazetidin-3-carbonitrile

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