[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

Base Information

Chemical Name:[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine
CAS No.:251940-36-0
Molecular Formula:C₁₂H₁₂Br₂N₃PS
Molecular Weight:421.095
Hs Code.:

Synonyms:[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

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Chemical Property of [2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

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Technology Process of [2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

There total 2 articles about [2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 251940-34-8
N¹,N¹-dimethyl-N²-(4-phenylthiazol-2-yl)formamidine

: 251940-36-0
[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

Guidance literature:: With phosphorus tribromide; In pyridine; at 20 ℃; for 4h;
DOI:10.1007/BF02495301

Reference yield:

: 2010-06-2
2-Amino-4-phenylthiazole

: 251940-36-0
[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / methanol / 5 h / Heating

2: 79 percent / PBr₃ / pyridine / 4 h / 20 °C

With phosphorus tribromide; In pyridine; methanol; 1: Substitution / 2: Substitution;
DOI:10.1007/BF02495301

Reference yield:

: 251940-36-0
[2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]dibromophosphine

: [2-(3-methyl-1,3-diazabut-1-enyl)-4-phenylthiazol-5-yl]tetraethyldiamidothiophosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / pyridine / 1.5 h

2: sulfur / benzene / 3 h / Heating

With sulfur; triethylamine; In pyridine; benzene; 1: Substitution / 2: Oxidation;
DOI:10.1007/BF02495301