N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

Base Information

Chemical Name:N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester
CAS No.:100856-23-3
Molecular Formula:C₂₆H₃₄N₂O₆
Molecular Weight:470.566
Hs Code.:

Synonyms:N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

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Technology Process of N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

There total 1 articles about N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 100856-22-2
N-<5-methyl-2-phenyl-4-t-butoxycarbonylpyrrol-3-yl>aminomethylenemalonic acid, diethyl ester

: 74-88-4
methyl iodide

: 100856-23-3
N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

Guidance literature:: With sodium methylate; In N,N-dimethyl-formamide; Ambient temperature; stirring overnight;
DOI:10.1002/jhet.5570220323

Reference yield: 91.0%

: 100856-23-3
N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

: 100856-24-4
N-<1,5-dimethyl-2-phenyl-4-carboxypyrrol-3-yl>methylaminomethylenemalonic acid diethyl ester

Guidance literature:: With methanesulfonic acid; for 0.166667h; Ambient temperature;
DOI:10.1002/jhet.5570220323

Reference yield:

: 100856-23-3
N-<2-phenyl-1,5-dimethyl-4-t-butoxycarbonylpyrrol-3-yl>methylaminomethylenemalonic acid, diethyl ester

: 100856-36-8
7-phenyl-1,5,6-trimethyl-1,4-dihydro-4-oxopyrrolo<3,4-b>pyridine-3-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / methane sulfonic acid / 0.17 h / Ambient temperature

2: 94 percent / polyphosphoric ester / 1.5 h / 100 - 110 °C

3: 75 percent / sodium hydroxide (1 percent) / methanol; H₂O / heating on a boiling water bath, 1 hr.,

With sodium hydroxide; polyphosphoric ester; methanesulfonic acid; In methanol; water;
DOI:10.1002/jhet.5570220323