3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Base Information

Chemical Name:3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione
CAS No.:1236069-66-1
Molecular Formula:C₂₆H₂₆Cl₂N₂O₂
Molecular Weight:469.411
Hs Code.:

Synonyms:3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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Chemical Property of 3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

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Technology Process of 3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

There total 3 articles about 3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 111-83-1
1-bromo-octane

: 84632-65-5,122390-98-1
3,6-bis(4-chlorophenyl)-2,5-dihydro-1,4-diketopyrrolo[3,4-c]pyrrole

: 1236069-66-1
3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: 3,6-bis(4-chlorophenyl)-2,5-dihydro-1,4-diketopyrrolo[3,4-c]pyrrole; With potassium tert-butylate; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h; Inert atmosphere;

1-bromo-octane; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.5012/bkcs.2014.35.2.659

Reference yield: 33.0%

: 111-83-1
1-bromo-octane

: 84632-65-5,122390-98-1
3,6-bis(4-chlorophenyl)-2,5-dihydro-1,4-diketopyrrolo[3,4-c]pyrrole

: 1236069-66-1
3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

: C₃₄H₄₂Cl₂N₂O₂

Guidance literature:: 3,6-bis(4-chlorophenyl)-2,5-dihydro-1,4-diketopyrrolo[3,4-c]pyrrole; With sodium t-butanolate; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

1-bromo-octane; In N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;
DOI:10.5012/bkcs.2010.31.04.1073

Reference yield:

: 623-03-0
4-Cyanochlorobenzene

: 1236069-66-1
3,6-bis(4-chlorophenyl)-2-octylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate; iron(III) chloride / tert-Amyl alcohol / 1.75 h / 110 °C / Inert atmosphere

1.2: 23 h / 110 °C / Inert atmosphere

2.1: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 3 h / 20 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere

With iron(III) chloride; potassium tert-butylate; In 1-methyl-pyrrolidin-2-one; tert-Amyl alcohol;
DOI:10.1080/15421406.2015.1075831