(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

Base Information

Chemical Name:(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene
CAS No.:1374149-00-4
Molecular Formula:C₂₆H₃₄O₄
Molecular Weight:410.554
Hs Code.:

Synonyms:(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

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Chemical Property of (((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

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Technology Process of (((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

There total 4 articles about (((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1374148-99-8
C₁₂H₂₂O₄

: 100-39-0
benzyl bromide

: 1374149-00-4
(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

Guidance literature:: C₁₂H₂₂O₄; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 1h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201400675

Reference yield:

: 2-(2,2-diethoxyethyl)-2-prop-2-ynylmalonic acid diethyl ester

: 1374149-00-4
(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / Inert atmosphere

2.1: sodium hydride / Inert atmosphere

2.2: Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride;
DOI:10.1021/ol300623j

Reference yield:

: 2032-35-1
Bromoacetaldehyde diethyl acetal

: 1374149-00-4
(((2-(2,2-diethoxyethyl)-2-(prop-2-yn-1-yl)propane-1,3-diyl)bis(oxy))bis(methylene))dibenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / Inert atmosphere

2.1: sodium hydride / Inert atmosphere

2.2: Inert atmosphere

3.1: lithium aluminium tetrahydride / Inert atmosphere

4.1: sodium hydride / Inert atmosphere

4.2: Inert atmosphere

With lithium aluminium tetrahydride; sodium hydride; potassium carbonate;
DOI:10.1021/ol300623j