benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside

Base Information

• Chemical Name: benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside
• CAS No.: 1442418-64-5
• Molecular Formula: C₇₃H₆₄O₂₁
• Molecular Weight: 1277.3

Synonyms:benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside

Chemical Property of benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside

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Technology Process of benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside

There total 1 articles about benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranoside (1372616-14-2) + 2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate (149707-75-5) → benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside (1442418-64-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 2h; Molecular sieve; Inert atmosphere;

DOI:10.1016/j.tet.2013.04.095

Reference yield: 89.0%

benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-hydroxyl-α-L-arabinopyranoside (1442418-64-5) + benzoyl chloride (98-88-4) → benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-O-benzoyl-α-L-arabinopyranoside (1375560-57-8)

Guidance literature:

With pyridine; at 0 - 20 ℃;

DOI:10.1016/j.tet.2013.04.095

upstream raw materials:

benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranoside

2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl trichloroacetimidate

Downstream raw materials:

benzyl-2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1→2)-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)]-3-O-benzoyl-α-L-arabinopyranoside

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