(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate

Base Information

• Chemical Name: (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate
• CAS No.: 1234550-51-6
• Molecular Formula: C₃₁H₅₂O₆Si
• Molecular Weight: 548.836

Synonyms:(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate

Chemical Property of (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate

Chemical Property:

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Technology Process of (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate

There total 1 articles about (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C31H54O6Si (1234550-62-9) → (2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate (1234550-51-6)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2010.04.039

Reference yield: 82.0%

(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate (1234550-51-6) + vinyl magnesium bromide (1826-67-1) → C33H56O6Si (1234550-65-2)

Guidance literature:

(2R,3S,4R)-2-(4-methoxybenzyloxy)-4-methylhex-5-en-3-yl (2R,3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-2,4,6-trimethyl-7-oxoheptanoate; vinyl magnesium bromide; In tetrahydrofuran; at 0 ℃;

With water; ammonium chloride; In diethyl ether;

DOI:10.1016/j.tet.2010.04.039

upstream raw materials:

C₃₁H₅₄O₆Si

Downstream raw materials:

C₃₃H₅₆O₆Si

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