(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

Base Information

Chemical Name:(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine
CAS No.:136778-88-6
Molecular Formula:C₂₂H₃₀N₂O
Molecular Weight:338.493
Hs Code.:

Synonyms:(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

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Technology Process of (2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

There total 1 articles about (2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 82101-54-0
1-<(S)-1-(benzyloxy)-4-methylpent-2-yl>-(3S,4R)-3-azido-4-phenylazetidin-2-one

: 136778-88-6
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

Guidance literature:: With chlorohydroalane; In diethyl ether; at 34 ℃; for 4h;
DOI:10.1021/jo00018a012

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 136778-88-6
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

: 136778-89-7
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-(acetylamino)azetidine

Guidance literature:: With pyridine; In chloroform; Ambient temperature;
DOI:10.1021/jo00018a012

Reference yield:

: 136778-88-6
(2R,3R)-1-<(S)-1-<(benzyloxy)methyl>-3-methylbutyl>-2-phenyl-3-aminoazetidine

: 136693-86-2
(2S,5S)-1-phenyl-2-(acetylamino)-5-(benzyloxymethyl)-7-methyl-4-azaoctane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / CHCl₃ / Ambient temperature

2: 100 percent / H₂ / 10percent Pd-C / methanol / 20 h / 25 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jo00018a012