ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

Base Information

Chemical Name:ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate
CAS No.:292632-42-9
Molecular Formula:C₁₈H₂₀N₄O₃
Molecular Weight:340.382
Hs Code.:

Synonyms:ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

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Chemical Property of ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

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Technology Process of ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

There total 1 articles about ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: ethyl 4-[1-methyl-2-(2,4-dimainofuro[2,3-d]pyrimidin-5-yl)ethenyl]benzoate

: 292632-42-9
ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

Guidance literature:: With hydrogen; 5percent Pd/C; In methanol; chloroform; N,N-dimethyl-formamide; at 20 ℃; for 5.5h; under 2327.23 Torr;
DOI:10.1021/jm000130i

Reference yield:

: 292632-42-9
ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

: 773043-69-9
(R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoic acid

Guidance literature:: With sodium hydroxide; In methanol; dimethyl sulfoxide; at 20 ℃; for 16h;
DOI:10.1021/jm000130i

Reference yield:

: 292632-42-9
ethyl (R,S)-4-[1-methyl-2-(2,4-diaminofuro[2,3-d]pyrimidin-5-yl)ethyl]benzoate

: C₂₁H₂₄N₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / methanol; dimethylsulfoxide / 16 h / 20 °C

2: Et₃N / dimethylformamide / 0.5 h / 0 °C

With sodium hydroxide; triethylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: Saponification / 2: Esterification;
DOI:10.1021/jm000130i