di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Base Information

Chemical Name:di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate
CAS No.:219591-91-0
Molecular Formula:C₃₂H₄₃F₂N₃O₈
Molecular Weight:635.706
Hs Code.:

di-tert-butyl N-<(4-<<N-(4-<bis<2-fluoroethyl>amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Synonyms:di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Chemical Property of di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

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Technology Process of di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

There total 10 articles about di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1027656-77-4
bis-(2-fluoro-ethyl)-(4-isocyanato-phenyl)-amine

: 180839-19-4
di-tert-butyl N-<(4-phenoxy)carbonyl>-L-glutamate

: 219591-91-0
di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: With dibutyltin(II) dilaurate; In toluene; for 12h; Ambient temperature;
DOI:10.1021/jm980425k

Reference yield:

: 18226-17-0
N,N-bis(2-hydroxyethyl)-4-nitroaniline

: 219591-91-0
di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h

2: Amberlyst 26 F^- / CHCl₃ / 72 h / Heating

3: 84 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 0.25 h

5: 69 percent / dibutyltin dilaurate / toluene / 12 h / Ambient temperature

With dmap; dibutyltin(II) dilaurate; Amberlyst 26 F^-; ammonium formate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; toluene;
DOI:10.1021/jm980425k

Reference yield:

: 219591-97-6
4-nitrobenzene

: 219591-91-0
di-tert-butyl N-<(4-<amino>phenyl)carbamoyloxy>methyl>phenoxy)carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / ammonium formate / 10 percent Pd/C / ethanol / 1.5 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 0.25 h

3: 69 percent / dibutyltin dilaurate / toluene / 12 h / Ambient temperature

With dibutyltin(II) dilaurate; ammonium formate; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm980425k