1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

Base Information

Chemical Name:1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide
CAS No.:1176166-44-1
Molecular Formula:Br*C₂₃H₃₁N₂
Molecular Weight:415.417
Hs Code.:

Synonyms:1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

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Technology Process of 1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

There total 2 articles about 1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 110-52-1
1,4-dibromo-butane

: 75105-48-5
N,N'-dimesitylformamidine

: 1176166-44-1
1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 125 ℃; for 2h; Neat (no solvent); Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.03.014

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 1176166-44-1
1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1 h / Reflux

2: potassium carbonate / acetonitrile / 48 h / Reflux

With potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1039/d0ob00036a

Reference yield: 75.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1176166-44-1
1,3-bis(2,4,6-trimethylphenyl)-4,5,6,7-tetrahydro-1H-1,3-diazepinium bromide

: AuBr(7-Mes)

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -78 - 20 ℃; for 6.5h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.inorgchem.9b00786