(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

Base Information

Chemical Name:(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide
CAS No.:1001438-61-4
Molecular Formula:C₂₃H₂₁ClN₂O₃S
Molecular Weight:440.95
Hs Code.:

Synonyms:(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

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Chemical Property of (E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

Chemical Property:

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Technology Process of (E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

There total 3 articles about (E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 180530-10-3
N-(3-iodophenyl)methanesulfonamide

: 1001438-72-7
(Z)-8-chloro-5-[1-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)propylidene]-5,11-dihydro-10-oxa-1-aza-dibenzo[a,d]cycloheptene

: 1001438-61-4
(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

Guidance literature:: With 3,5-dimethoxyphenol; potassium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 80 ℃; for 18h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 1001438-73-8
(E)-3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenylamine

: 124-63-0
methanesulfonyl chloride

: 1001438-61-4
(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 6.9 - 20 ℃;

Reference yield:

: (E)-3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)propyl]phenylamine, ditoluenesulfonic acid salt

: 124-63-0
methanesulfonyl chloride

: 1001438-61-4
(E)-N-{3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)-propyl]-phenyl}-methanesulfonamide

Guidance literature:: (E)-3-[1-(8-chloro-11H-10-oxa-1-aza-dibenzo[a,d]cyclohepten-5-ylidene)propyl]phenylamine, ditoluenesulfonic acid salt; With sodium carbonate; In dichloromethane; water;

methanesulfonyl chloride; With pyridine; In dichloromethane; at 20 ℃;