methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

Base Information

Chemical Name:methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate
CAS No.:1096143-69-9
Molecular Formula:C₄₇H₅₄O₉Si
Molecular Weight:791.026
Hs Code.:

Synonyms:methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

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Technology Process of methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

There total 1 articles about methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1096143-66-6
methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

: 1096143-69-9
methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

Guidance literature:: With sodium; In methanol; at 0 ℃; for 0.5h;
DOI:10.1016/j.carres.2008.08.030

Reference yield: 90.0%

: 1096143-69-9
methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

: methyl (2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/j.carres.2008.08.030

Reference yield: 89.0%

: 1096143-69-9
methyl 3-O-tert-butyldiphenylsilyl-(2R)-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-2,3-dihydroxypropanoate

: 1400562-33-5
phenyl 2,3-di-O-benzyl-4,6-di-O-chloroacetyl-1-thio-β-D-galactopyranoside

: 1448042-67-8
methyl (2R)-3-O-tert-butyldiphenylsilyl-2-O-[2,3-di-O-benzyl-4,6-di-O-chloroacetyl-α-D-galactopyranosyl-(1→6)-2,3,4-tri-O-benzyl-1-O-α-D-glucopyranosyl]-2,3-dihydroxypropanoate

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.25h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2013.06.038