(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

Base Information

Chemical Name:(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate
CAS No.:697288-43-0
Molecular Formula:C₂₀H₃₁NO₃
Molecular Weight:333.471
Hs Code.:

Synonyms:(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

Chemical Property:

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Technology Process of (R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

There total 7 articles about (R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1358759-94-0
(S,E)-1-phenylbut-2-enyl diisopropylcarbamate

: 67-64-1
acetone

: 697288-43-0
(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

Guidance literature:: (S,E)-1-phenylbut-2-enyl diisopropylcarbamate; With n-butyllithium; In 4-methyl-morpholine; hexane; at -50 ℃; for 0.0833333h;

acetone; In 4-methyl-morpholine; hexane; at -50 ℃; for 0.166667h; optical yield given as %ee;
DOI:10.1002/ejoc.201100970

Reference yield:

: 1358759-94-0
(S,E)-1-phenylbut-2-enyl diisopropylcarbamate

: 67-64-1
acetone

: 697288-43-0
(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

: 697288-44-1
(S,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

Guidance literature:: (S,E)-1-phenylbut-2-enyl diisopropylcarbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -50 ℃; for 0.0833333h;

acetone; In tetrahydrofuran; hexane; at -50 ℃; for 0.166667h; optical yield given as %ee;
DOI:10.1002/ejoc.201100970

Reference yield:

: 1358759-94-0
(S,E)-1-phenylbut-2-enyl diisopropylcarbamate

: 67-64-1
acetone

: 1358760-08-3
(R,E)-1-phenylbut-2-enyl diisopropylcarbamate

: 697288-43-0
(R,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

: 697288-44-1
(S,Z)-4-hydroxy-3,4-dimethyl-1-phenylpent-1-en-1-yl diisopropylcarbamate

Guidance literature:: (S,E)-1-phenylbut-2-enyl diisopropylcarbamate; With n-butyllithium; In hexane; tert-butyl methyl ether; at -50 ℃; for 0.0833333h;

acetone; In hexane; tert-butyl methyl ether; at -50 ℃; for 0.166667h;
DOI:10.1002/ejoc.201100970