.beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate

Base Information

Chemical Name:.beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate
CAS No.:228115-58-0
Molecular Formula:C₂₂H₂₅O₉P
Molecular Weight:464.409
Hs Code.:

Synonyms:.beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate

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Chemical Property of .beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate

Chemical Property:

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Technology Process of .beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate

There total 5 articles about .beta.-D-Galactopyranose, 1,6-anhydro-, 3-acetate 2-bis(phenylmethyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52579-97-2
1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose

: 228115-58-0
3-O-acetyl-1,6-anhydro-β-D-galactopyranose 2-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / butyllithium / tetrahydrofuran; hexane / 48 h / -60 - 20 °C

2: 50 percent / aq. HCl / tetrahydrofuran / 1 h / Heating

3: pyridine

With pyridine; hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane; 1: Esterification / 2: Hydrolysis / 3: Acetylation;
DOI:10.1016/S0040-4020(99)00327-0

Reference yield:

: 228115-52-4
1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose 2-(dibenzyl phosphate)

: 228115-58-0
3-O-acetyl-1,6-anhydro-β-D-galactopyranose 2-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / aq. HCl / tetrahydrofuran / 1 h / Heating

2: pyridine

With pyridine; hydrogenchloride; In tetrahydrofuran; 1: Hydrolysis / 2: Acetylation;
DOI:10.1016/S0040-4020(99)00327-0