1,10-undecadien-6-one oxime O-benzyl ether

Base Information

• Chemical Name: 1,10-undecadien-6-one oxime O-benzyl ether
• CAS No.: 156370-42-2
• Molecular Formula: C₁₈H₂₅NO
• Molecular Weight: 271.403
• Mol file: 156370-42-2.mol

Synonyms:1,10-undecadien-6-one oxime O-benzyl ether

Chemical Property of 1,10-undecadien-6-one oxime O-benzyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,10-undecadien-6-one oxime O-benzyl ether

There total 1 articles about 1,10-undecadien-6-one oxime O-benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

undeca-1,10-dien-6-one (69856-81-1) + O-benzylhydoxylamine hydrochloride (2687-43-6) → 1,10-undecadien-6-one oxime O-benzyl ether (156370-42-2)

Guidance literature:

With sodium acetate; In water; acetonitrile; at 20 ℃; for 8h;

DOI:10.1016/S0040-4020(01)01118-8

Reference yield:

1,10-undecadien-6-one oxime O-benzyl ether (156370-42-2) → cis-2-(4-pentenyl)-6-[(phenylseleno)methyl]piperidine

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 16 h / 20 °C

2: 0.78 g / sodium borohydride / methanol; CH₂Cl₂ / 1 h / 20 °C

With sodium tetrahydroborate; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4020(01)01118-8

Reference yield:

1,10-undecadien-6-one oxime O-benzyl ether (156370-42-2) → trans-2-(4-pentenyl)-6-[(phenylseleno)methyl]piperidine

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 16 h / 20 °C

2: 0.11 g / sodium borohydride / methanol; CH₂Cl₂ / 1 h / 20 °C

With sodium tetrahydroborate; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4020(01)01118-8

upstream raw materials:

undeca-1,10-dien-6-one

O-benzylhydoxylamine hydrochloride