4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Base Information

Chemical Name:4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine
CAS No.:119694-66-5
Molecular Formula:C₃₆H₆₀N₂O₉SSi₂
Molecular Weight:753.117
Hs Code.:

Synonyms:4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

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Chemical Property of 4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

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Technology Process of 4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

There total 1 articles about 4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 119694-66-5
4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With tetrabutylammomium bromide; sodium carbonate; In dichloromethane; water; for 15h; Ambient temperature;
DOI:10.1021/jo00271a015

Reference yield: 6.0%

: 119694-66-5
4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 69304-42-3
3',5'-O-[(1,1,3,3-tetraisopropyl)-1,3-disiloxanediyl]cytidine

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With ammonium hydroxide; In 1,4-dioxane; for 4h; Ambient temperature;
DOI:10.1021/jo00271a015

Reference yield:

: 119694-66-5
4-O-<(2,4,6-triisopropylphenyl)sulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 108782-95-2
N³-(4-methylbenzoyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: Multi-step reaction with 2 steps

1: 6 percent / conc. aq. NH₃ / dioxane / 4 h / Ambient temperature

2: 1.) Na₂CO₃, tetrabutylammonium bromide / 1.) CH₂Cl₂, H₂O, RT, 45 min, 2.) 1,2-dichloroethane, 60 deg C, 45 min

With ammonium hydroxide; tetrabutylammomium bromide; sodium carbonate; In 1,4-dioxane;
DOI:10.1021/jo00271a015