tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

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Chemical Name:tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate
CAS No.:1030827-14-5
Molecular Formula:C₂₈H₃₉NO₆
Molecular Weight:485.621
Hs Code.:

Synonyms:tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

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Chemical Property of tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

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Technology Process of tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

There total 1 articles about tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1030827-32-7
(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

: 1030827-14-5
tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 11h; Inert atmosphere; Reflux;
DOI:10.1021/ol8004672

Reference yield: 59.0%

: 1030827-14-5
tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

: 1030827-15-6
(5S,6S)-6-((E,3R,4R)-6-(4-methoxybenzyloxy)-3-(2-(butoxycarbonyl)aminoethyl)-3,4-dihydroxyhex-1-enyl)-5-ethyl-5,6-dihydropyran-2-one

: 1030827-33-8
C₂₈H₄₁NO₈

Guidance literature:: With potassium osmate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 10h; diastereoselective reaction;
DOI:10.1021/ol8004672

Reference yield: 59.0%

: 1030827-14-5
tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

: 1030827-15-6
(5S,6S)-6-((E,3R,4R)-6-(4-methoxybenzyloxy)-3-(2-(butoxycarbonyl)aminoethyl)-3,4-dihydroxyhex-1-enyl)-5-ethyl-5,6-dihydropyran-2-one

: C₂₈H₄₁NO₈

Guidance literature:: With methanesulfonamide; AD-mix β; In water; tert-butyl alcohol; at 0 ℃; for 10h; regioselective reaction;
DOI:10.1055/s-0029-1216930