(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

Base Information

Chemical Name:(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate
CAS No.:1030827-32-7
Molecular Formula:C₃₀H₄₃NO₆
Molecular Weight:513.675
Hs Code.:

Synonyms:(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

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Chemical Property of (3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

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Technology Process of (3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

There total 1 articles about (3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1030827-13-4
tert-butyl [(3E,4E,6S,7S)-7-ethyl-6-hydroxy-3-{3-[(4-methoxybenzyl)oxy]propylidene}nona-4,8-dien-1-yl]carbamate

: 814-68-6,25189-84-8
acryloyl chloride

: 1030827-32-7
(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ol8004672

Reference yield: 77.0%

: 1030827-32-7
(3S,4S,5E,7E)-7-{2-[(tert-butoxycarbonyl)amino]ethyl}-3-ethyl-10-[(4-methoxybenzyl)oxy]deca-1,5,7-trien-4-yl acrylate

: 1030827-14-5
tert-butyl {(3E)-3-{(E)-2-[(2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl]vinyl}=6=[(4-methoxybenzyl)oxy]hex-3-en-1yl}carbamate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 11h; Inert atmosphere; Reflux;
DOI:10.1021/ol8004672