(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

Base Information

Chemical Name:(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt
CAS No.:203053-87-6
Molecular Formula:C₂HF₃O₂*C₁₂H₁₆N₂O₃
Molecular Weight:350.295
Hs Code.:

Synonyms:(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

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Chemical Property of (S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

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Technology Process of (S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

There total 4 articles about (S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 203053-87-6
(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

2: dichloromethane

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201501850

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 203053-87-6
(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 0 - 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C

3: dichloromethane

With thionyl chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201501850

Reference yield:

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 203053-87-6
(S)-methyl 2-(2-aminoacetamido)-3-phenylpropanoate trifluoroacetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C

2: dichloromethane / 3 h / 0 - 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.bmc.2019.07.044