ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

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Chemical Name:ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate
CAS No.:869296-12-8
Molecular Formula:C₁₇H₁₆N₂O₄S
Molecular Weight:344.391
Hs Code.:

Synonyms:ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

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Chemical Property of ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

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Technology Process of ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

There total 6 articles about ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 869296-11-7
ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

: 100-51-6,185532-71-2
benzyl alcohol

: 869296-12-8
ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 10 - 35 ℃; for 0.166667h;

ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate; at 10 - 35 ℃; for 1h; Further stages;

Reference yield: 16.0%

: 869296-11-7
ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

: 64-17-5
ethanol

: 100-51-6,185532-71-2
benzyl alcohol

: 869296-12-8
ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.166667h;

ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

ethanol; Further stages;
DOI:10.1016/j.bmc.2014.07.025

Reference yield:

: 869296-11-7
ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

: 100-51-6,185532-71-2
benzyl alcohol

: 869296-12-8
ethyl 4-oxo-5-{[(phenylmethyl)oxy]methyl}-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate

: C₁₅H₁₂N₂O₄S

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.166667h;

ethyl 5-(bromomethyl)-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-2-carboxylate; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2014.07.025