1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Base Information

Chemical Name:1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone
CAS No.:1269792-90-6
Molecular Formula:C₂₅H₂₁ClN₄OS
Molecular Weight:460.987
Hs Code.:

Synonyms:1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Suppliers and Price of 1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

There total 3 articles about 1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1269792-63-3
1-(2-p-chlorobenzylidenehydrazinyl)-3-thioxo-5,6,7,8-tetrahydroisoquinoline-4-carbonitrile

: 70-11-1
α-bromoacetophenone

: 1269792-90-6
1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Guidance literature:: With sodium acetate; In ethanol; for 2h; Reflux;
DOI:10.1016/j.ejmech.2010.11.036

Reference yield:

: 1269792-60-0
1-hydrazino-3-thioxo-5,6,7,8-tetrahydroisoquinoline-4-carbonitrile

: 1269792-90-6
1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 2.08 h / Reflux

2: sodium acetate / ethanol / 2 h / Reflux

With piperidine; sodium acetate; In ethanol;
DOI:10.1016/j.ejmech.2010.11.036

Reference yield:

: 50706-78-0
2,3,5,6,7,8-hexahydro-1-morpholin-4-yl-3-thioxo-isoquinoline-4-carbonitrile

: 1269792-90-6
1-(2-p-chlorobenzylidenehydrazinyl)-4-cyano-5,6,7,8-tetrahydroisoquinoline-3-sulfanylacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 2 h / Reflux

2: piperidine / ethanol / 2.08 h / Reflux

3: sodium acetate / ethanol / 2 h / Reflux

With piperidine; sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2010.11.036