(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

Base Information

Chemical Name:(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol
CAS No.:405234-97-1
Molecular Formula:C₂₅H₂₅NO₂
Molecular Weight:371.479
Hs Code.:

Synonyms:(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

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Chemical Property of (4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

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Technology Process of (4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

There total 1 articles about (4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 82659-84-5
(4S,5S)-5-methyl-2-phenyl-4,5-dihydro-oxazole-4-carboxylic acid methyl ester

: 6921-34-2
benzylmagnesium chloride

: 405234-97-1
(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

Guidance literature:: In diethyl ether; at -78 - 20 ℃; for 4h;
DOI:10.1002/1615-4169(200201)344:1<40::AID-ADSC40>3.0.CO;2-7

Reference yield: 62.0%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 405234-97-1
(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

: (4S,5S)-O-[1-benzyl-1-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-2-phenylethyl] diphenylphosphinite

: Diphenyl-phosphinic acid 1-benzyl-1-((4S,5S)-5-methyl-2-phenyl-4,5-dihydro-oxazol-4-yl)-2-phenyl-ethyl ester

Guidance literature:: (4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In pentane; at -78 - 20 ℃; for 1h;

chloro-diphenylphosphine; In pentane; at 0 - 20 ℃; for 5h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/1615-4169(200201)344:1<40::AID-ADSC40>3.0.CO;2-7

Reference yield:

: 36042-94-1
bis(o-tolyl)chlorophosphine

: 405234-97-1
(4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol

: C₃₉H₃₈NO₂P

Guidance literature:: (4S,5S)-2-(5-methyl-2-phenyl-4,5-dihydrooxazol-4-yl)-1,3-diphenylpropan-2-ol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In pentane; at -78 - 20 ℃;

bis(o-tolyl)chlorophosphine; In pentane; at 0 - 20 ℃; Further stages.;
DOI:10.1002/1615-4169(200201)344:1<40::AID-ADSC40>3.0.CO;2-7