(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

Base Information

Chemical Name:(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester
CAS No.:932040-83-0
Molecular Formula:C₁₅H₁₈F₃NO₂
Molecular Weight:301.309
Hs Code.:

Synonyms:(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

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Chemical Property of (S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

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Technology Process of (S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

There total 4 articles about (S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.8%

: C₁₅H₁₈F₃NO₂

: 932040-83-0
(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In hexane; at 75 ℃; for 9h;
DOI:10.1016/j.jfluchem.2006.04.003

Reference yield:

: 197638-60-1
(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

: 932040-83-0
(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

: (R)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 75 ℃; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo9710238

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 932040-83-0
(S)-4,4,4-Trifluoro-3-[1-phenyl-eth-(E)-ylideneamino]-butyric acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: DBU / 24 h / 75 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene;
DOI:10.1021/jo9710238