(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

Base Information

Chemical Name:(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate
CAS No.:197638-60-1
Molecular Formula:C₁₅H₁₈F₃NO₂
Molecular Weight:301.309
Hs Code.:

Synonyms:(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

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Technology Process of (+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

There total 2 articles about (+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 108-21-4
Isopropyl acetate

: 2,2,2-trifluoro-N-(1-phenyl-ethyl)-acetimidoyl chloride

: 197638-60-1
(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

Guidance literature:: Isopropyl acetate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -50 ℃; for 1.5h;

2,2,2-trifluoro-N-(1-phenyl-ethyl)-acetimidoyl chloride; In tetrahydrofuran; hexane; at -78 ℃; Further stages.;
DOI:10.1021/jo025621k

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 175230-50-9
isopropyl 4,4,4-trifluoro-3-oxobutanoate

: 197638-60-1
(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

Guidance literature:: DOI:10.1021/jo9710238

Reference yield: 98.0%

: 197638-60-1
(+)-isopropyl (Z)-4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]-2-butenoate

: isopropyl 4,4,4-trifluoro-3-[(1S)-1-phenylethylamino]butanoate

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; methanol; water; at 0 ℃; for 1.5h;
DOI:10.1021/jo025621k