4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

Base Information

Chemical Name:4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile
CAS No.:1290601-89-6
Molecular Formula:C₃₃H₃₈N₄O₄S₆
Molecular Weight:747.085
Hs Code.:

4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

Synonyms:4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

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Chemical Property of 4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

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Technology Process of 4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

There total 1 articles about 4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1023911-63-8
N,N′-((propane-1,3-diylbis(sulfanediyl))bis(ethane-2,1-diyl))bis(4-methylbenzenesulfonamide)

: 1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene

: 1290601-89-6
4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

Guidance literature:: N,N′-((propane-1,3-diylbis(sulfanediyl))bis(ethane-2,1-diyl))bis(4-methylbenzenesulfonamide); With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 2h; Inert atmosphere;

1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene; In N,N-dimethyl-formamide; at 50 ℃; for 147h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2011.01.035

Reference yield: 59.0%

: 1290601-89-6
4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

: C₁₃₂H₁₅₂N₁₆O₁₆PbS₂₄

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; lead(II) oxide; at 175 ℃; for 0.1h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.jorganchem.2011.01.035

Reference yield: 59.0%

: 108-01-0
2-(N,N-dimethylamino)ethanol

: 1290601-89-6
4,14-bis[(4-methylphenyl)sulfonyl]-3,4,5,6,9,10,13,14,15,16-decahydro-2H,8H,12H-1,17,7,11,4,14-benzotetrathiadiazacyclononadecin-19,20-dicarbonitrile

: lead(II) oxide

: lead(II) tetrathiadi(aza(4-methylphenyl)sulfonyl)phthalocyanine

Guidance literature:: In ethanol; other Radiation; Schlenk techniques under N2 used, mixt. of (NC)2C17H24S4N2(Ts)2 (0.13 mmol), PbO (0.033 mmol) and (2-methylamino)ethanol (2 ml) irradiated at 175°C, 350W for 9 min, cooled to room temp., refluxed with EtOH; filtered, washed with hot ethanol and methanol, dried in vac. over P2O5,chromd. (silica gel, CHCl3:MeOH (9:1)); elem. anal.;
DOI:10.1016/j.jorganchem.2011.01.035