1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Base Information

Chemical Name:1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone
CAS No.:90158-33-1
Molecular Formula:C₂₄H₃₁NO₅
Molecular Weight:413.514
Hs Code.:

Synonyms:1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

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Chemical Property of 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Chemical Property:

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Technology Process of 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

There total 4 articles about 1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 408313-93-9
1-(2-benzyloxy-3,4-dimethoxyphenyl)-2-<3-(1,1-ethylenedioxyethyl)piperidino>ethanol

: 90158-33-1
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Guidance literature:: With hydrogenchloride; In water; at 40 ℃; for 2h;
DOI:10.1248/cpb.33.5316

Reference yield:

: 89680-89-7
1-(2-benzyloxy-3,4-dimethoxyphenacyl)-3-(1,1-ethylenedioxyethyl)pyridinium bromide

: 90158-33-1
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) NaBH₄ / 1.) 50percent aq. EtOH, Adams catalyst (PtO₂*H₂O), 1 atm, room temp., 18 h

2: 98 percent / HCL aq. / 2 h / 40 °C

With hydrogenchloride; sodium tetrahydroborate; hydrogen;

Reference yield:

: 55676-25-0
3-(2-methyl-[1,3]dioxolan-2-yl)-pyridine

: 90158-33-1
1-<2-(2-benzyloxy-3,4-dimethoxyphenyl)-2-hydroxyethyl>-3-piperidyl methyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / benzene / 5 h / Ambient temperature

2: 1.) H₂; 2.) NaBH₄ / 1.) Adams catalyst / 1.) ethanol/water, 18 h, room temperature; 2.) ethanol/water, room temperature

3: 98 percent / 1N HCl / H₂O / 2 h / 40 °C

With hydrogenchloride; sodium tetrahydroborate; hydrogen; platinum(IV) oxide; In water; benzene;
DOI:10.1248/cpb.33.5316